ISSN 2738-0971 | eISSN 2738-1013

Anja Jokić

Faculty of Natural Science and Mathematics, Kosovska Mitrovica

Articles

Open Access Original Scientific Paper

PREPARATION OF SILVER AND COPPER NANOPARTICLES IN PRESENCE OF ASCORBIC ACID AND INVESTIGATION OF THEIR ANTIBACTERIAL ACTIVITY

In this study, we present a synthesis of silver and copper nanoparticles (NPs) using ascorbic acid as stabilizing and sodium borohydride as reducing agents, respectively. Four colloidal dispersions were obtained, two of them additionally stabilized by gelatin. They were characterized by UV-Vis, AFM, DLS and zeta potential measurements. The size of both silver and copper NPs, determined by AFM measurements, was 10 nm before, and 15 nm after stabilization with gelatin. Antibacterial activity of synthesized NPs was tested using series of gram positive and gram negative bacteria. It was found that Ag and Cu NPs showed antibacterial activity in all cases.

Open Access

CHARACTERIZATION OF NEW SYNTHESIZED Fe2O3 NANOPARTICLES AND THEIR APPLICATION AS DETECTION SIGNAL AMPLIFIERS IN HERBICIDE BENTAZONE ELECTROANALYTICAL DETERMINATION

The iron oxide nanoparticles (Fe2O3 NPs) were synthesized from two different iron salts by solid-state synthesis method. The synthesized powder of Fe2O3 NPs is soluble in water, and the colloidal dispersion was characterized by TEM, FTIR, UV-Vis spectroscopy and zeta potential measurements. Obtained NPs are spherical in shape with narrow particle size distribution and an average diameter of 3 nm. Further, the possible application of Fe2O3 NPs was proposed, due to significant electroanalytical signal amplification in the determination of herbicide bentazone in natural river water.

Open Access

A MINI-REVIEW OF ELECTROANALYTICAL METHODS FOR PESTICIDES QUANTIFICATION

This review paper shows the progress made in the last five years in electrochemical methods applied for the purpose of detection and quantification of pesticides - nowadays the most serious pollutants of the environment. Most pesticides can be successfully analyzed by chromatographic techniques, but because of high prices and immobility of the apparatus, the complexity of the method and the necessary special preparation of the samples, electrochemical methods have been recognized as an excellent alternative solution due to their advantages in speed, economy, simplicity and no exhaustive sample preparation. As the main limitation for use of this methods is electrochemical inactivity of many pesticides, this paper gives the essence of all elctroanalytical methods for pesticide quantification applied in last period, with an overview of the electrode materials and modifiers applied in a purpose to enhance analytical procedures application and characteristics of electrochemical sensors.